Dynamic Recrystallization in the Shear Bands of Tungsten Heavy Alloy Processed by Hot-Hydrostatic Extrusion and Hot Torsion

Hot-hydrostatic extrusion and hot torsion (HE+HT) were applied to the processing of the as-sintered tungsten heavy alloy (WHA). The dynamic mechanical properties of the WHA processed by HE+HT and the microstructural evolution within adiabatic shear band (ASB) were systematically investigated. The results show that the WHA susceptibility to ASB is much improved, and localized shear bands can be formed in specimens. TEM analysis of ASB shows that the multiplication and rearrangement of dislocation play dominate roles in the dynamic recrystallization (DRX) process within ASB of WHA, and the nano-scaled equiaxed-recrystallized grains within ASB can be formed via repeating the processes including dislocation multiplication, dislocation rearrangement and dislocation annihilation. The investigation result of observed DRX of the WHA firmly supports the rotational dynamic recrystallization (RDR) mechanism in metals.     

脉冲式红外热波无损检测的热激励均匀性

热激励技术是主动式脉冲红外热波无损检测的关键技术之一。热激励的均匀性不仅直接影响红外探伤热图的品质,而且关系到提取被测物体表面温度差的精度,进而影响到后期的缺陷定量识别。利用照明设计软件TracePro,对加热光源的空间特性、照度分布特性以及多灯阵列和遮罩设计进行了实体仿真分析。结果表明,多灯阵列有助于提高被照射面上的照度均匀性,同时采用遮罩也可以大幅聚光,在被照射面上形成均匀辐射。多次仿真均取得了较好的效果,为后期热激励的硬件设计奠定了基础,具有一定的应用价值。     

Oxygen doped Ge crystals Czochralski-grown from the B2O3-fully-covered melt

Local vibrations of oxygen in Ge crystals grown from a melt fully covered by B₂O₃ were evaluated by Fourier-transform infrared spectroscopy. Ge single crystals containing oxygen were grown by the Czochralski method under various growth conditions. Oxygen concentrations in the crystals were determined to be in the range between 8.5 × 10¹⁵ and 5.5 × 10¹⁷ cm⁻³ from the infrared absorption at 855 cm⁻¹ originating in local vibration of Ge-O_i-Ge quasi-molecules. Absorption peaks relating to GeO_x, SiO_x and Si-O_i-Si were not detected in the as-grown crystals. The calibration coefficient for determining oxygen concentration in Ge crystals from the absorption peak intensity at 1264 cm⁻¹ was estimated to be 1.15 × 10¹⁹ cm⁻².     

用于焦平面测试系统的高效高精度数据采集方法与实现

通过分析焦平面测试中各种性能参数对数据要求的特点,提出了一种区别于传统的高效数据采集方法,并采用ADI最新发布的16位高性能ADC,设计了基于该方法的高效高精度采集系统.通过内嵌的“RMS硬件算法”和外部SRAM的特殊组合,在兼容传统测试系统的同时,大大提高了系统的测试效率.经碲镉汞(HgCdTe)型640×512(1...     

红外伪装篷布的制备与测试

通过对红外隐身理论的研究,选择分散黄E-3RL、藏青S-2G、蓝E-4R、黑S-2BL、金黄ETD、翠蓝ETD等染料作为主要染料,配以其它常用染色助剂,对军绿和林地迷彩以及沙漠迷彩进行配色,实现了对可见光和近红外的隐身。并通过金属镀膜空心玻璃微珠与印花浆、增稠剂调成整理液对蓬布进行涂层整理,得到具有热红外伪装能力的蓬布。通过野外实地测试得到显著的效果。     

一种红外图像增强的新方法

结合红外图像的成像特点,采用各种图像,增强算法对红外图像进行处理,分别实现了对比度提高、抑制噪声及增强边缘的效果。在此基础上,根据不同算法可实现的效果,提出了一种可将几种算法的优点融合为一体的混合算法。这种算法进一步提高了图像的视觉效果。     

Gasmet便携式傅里叶变换红外气体分析仪及其在环境应急监测中的应用

本文主要介绍了芬兰Gasmet Technologies Oy公司生产的GASMET FTIR Dx4020便携式傅里叶变换红外气体分析仪。包括它的工作原理和多组分同时定性、定量测定原理,以及随机携带的Calcmet中文智能软件功能、仪器内部配置。出厂进行一次初始标定后,无需再次标定等性能特点,最后从仪器的多组分定性、现场定量、连续监测三个特点列举了本仪器在环境应急监测中的应用事例     

Evaluation of Low‐Cost Separators for Increased Power Generation in Single Chamber Microbial Fuel Cells with Membrane Electrode Assembly

We compared novel size‐selective separators, namely the textile fabrics of polyphenylene sulfide (PPS) and sulfonated polyphenylene sulfide (S‐PPS), and the nonwoven fabrics of polypropylene80 (PP 80) and PP 100, with commonly used ion exchange separators (Nafion 117 and cation exchange membane‐7000; CMI‐7000) in terms of power generation, oxygen diffusion, and biofilm formation in a single chamber microbial fuel cell. Size‐selective separators exhibited more power generation than ion selective separators. MFC operation with size‐selective separators generated power output ranging 0.407 to 0.591 V (1000 Ω), whereas with Nafion it was 0.272 V. In polarization analysis, S‐PPS resulted in the highest power density of 190 mW/m², whereas it was 24 mW/m² with Nafion‐117. Size selective separators showed similar or higher proton conductivity than Nafion 117. Oxygen mass transfer coefficients of size‐selective separators (K_O = 3.7 ∼ 7.5 × 10⁻⁵) were lower or similar to Nafion (K_O = 7.5 × 10⁻⁵). Fourier‐transform infrared spectroscopy and scanning electron microscopy analysis revealed that all separators (PP80, S‐PPS, and Nafion) contained proteins or carbon chain compounds after 300‐day operation, and however, Nafion 117 seems to be more susceptible to biofouling than the other separators.     

高含硫气田快开盲板密封材料耐硫性能评价与失效分析

以普光油气田现场所用快开盲板密封橡胶为研究对象,进行了室内模拟H2S/CO2环境的腐蚀实验,分析了其腐蚀前后的外观、力学性能、微观结构及红外光谱的变化,推断了快开盲板橡胶密封材料的腐蚀机理。结果表明,腐蚀后密封橡胶材料的力学性能损失严重,主要是由三种原因造成的,一是加压时溶解在密封材料基体内部的气体在减压的过程中膨胀而形成裂纹;二是在腐蚀过程中基体内部的填料与氟橡胶基体之间脱粘;三是在腐蚀过程中硫化氢与主链共轭双键反应,使密封材料的交联点被破坏。     

Optimization of infrared radiation cure process parameters for glass fiber reinforced polymer composites

Elevated temperature post curing is one of the most critical step in the processing of polymer composites. It ensures that the complete cross-linking takes place to produce the targeted properties of composites. In this work infrared radiation (IR) post curing process for glass fiber reinforced polymer composite laminates is studied as an alternative to conventional thermal cure. Distance from the IR source, curing schedule and volume of the composite were selected as the IR cure parameters for optimization. Design of experiments (DOE) approach was adopted for conducting the experiments. Tensile strength and flexural strength of the composite laminate were the responses measured to select the final cure parameters. Analysis of variance (ANOVA), surface plots and contour plots clearly demonstrate that the distance from the IR source and volume of the composite contribute nearly 70% to the response functions. This establishes that polymer composites cured using IR technique can achieve the same properties using only 25% of the total time compared to that of conventional thermal curing.